Kamis, 17 Juli 2014



P-001
Complex Paternity investigations: The need for more genetical information

Abrantes D1, Pontes ML1, Lima G1, Cainé L1, Pereira MJ1, Matos P1, Pinheiro MF1,2

1Instituto Nacional de Medicina Legal – Delegação do Porto
2Faculdade de Ciências da Saúde – Universidade Fernando Pessoa

In the past few years our laboratory has been registering a raising demand of difficult parentage investigations, namely those performed in the absence of the putative father’s genetical data. Due to the also increasing complexity of the aforementioned investigation cases themselves, the results provided by the routinely used commercial kits AmpFSTR® Identifiler (Applied Biosystems) and Powerplex® 16 (Promega), in our laboratory, even in conjunction with the complementary commercial kit Powerplex® ES Monoplex System (SE33), are no longer always satisfactory. Therefore, there is an urgent need for more (preferably) easily- and rapidly-analysable markers. In this sense, our laboratory resorted to the long-time commercialized kit Gene Print® Fluorescent STR Systems FFFL Multiplex (Promega), which allows for the co-amplification of four more STR-loci (F13A01, FES/FPS, F13B e LPL) and, thus, for the acquisition of the required supplementary genetical data. In this work, we describe several cases to whose solution the FFFL data were crucial. We also report the allelic frequencies and some parameters of forensic interest, relative to FFFL loci, for the Northern Portuguese population.

Contact: Biologia@dpinml.mj.pt


P-002
Accurate mtDNA mixture quantification using the Pyrosequencing technology

Allen M, Nilsson M, Andréasson H
Department of Genetics and Pathology, Rudbeck Laboratory, Uppsala University, Sweden

Analysis of mtDNA variation using Sanger sequencing does not allow accurate quantification of mtDNA mixtures. Thus, a method to determine the specific mixture ratios in samples displaying heteroplasmy, consisting of DNA contribution from several individuals or containing contamination would be valuable. In this study, a novel quantification system for mtDNA mixture analysis is described. The assay is based on pyrosequencing technology, in which the linear relationship between incorporated nucleotides and released light allows accurate quantification. The routinely applied Sanger sequence analysis of mtDNA is robust and in most cases successful due to the high copy number of mtDNA per cell. However, occasionally samples show a DNA mixture as a consequence of multiple contributors, heteroplasmy or contamination. In contrast to STR analysis, quantification of mixed samples based on mtDNA sequence analysis is not feasible using the current sequencing methodology. The ABI PRISMÒ BigDyeTM Primer Cycle Sequencing Ready Reaction Kit (Applied Biosystems, Foster City, CA) is commonly used for mtDNA analysis. Although this chemistry easily and effectively determines the sequence in single source samples, the uneven peak heights and sequence-dependent variation in dideoxynucleotide incorporation efficiency prevent quantification of mixtures. Thus mixtures can be detected and visualised using Sanger sequencing, but the information cannot be used to determine the exact quantities of the different mitochondrial types and in most cases the results are called as inconclusive. Resolution of mtDNA mixtures has been demonstrated previously using alternative technologies such as cloning and denaturing high-performance liquid chromatography. However, in order to resolve and accurately quantify multiple individuals contributing to a sample in equal or unequal ratios, an easy to use quantitative assay would be useful. Pyrosequencing is a technology based on the release of pyrophosphate during strand elongation, producing light. The light signal is proportional to incorporated nucleotides, allowing allele quantification utilising PSQTM96MA SNP Software (Version 2.02, Biotage, Uppsala, Sweden). The allele quantification capability has been previously used in a number of studies, including allele frequency measurements in pooled DNA samples and quantitative analysis of methylation status at CpG islands. Other studies involve gene copy number measurements and determination of allele-specific transcript expression. In this study, a subset of PCR fragments previously developed for a fast and simple pyrosequencing analysis of variation in the mtDNA control and coding region, were used for pyrosequencing based quantification. Seven polymorphic sites, three in the control region and four in the coding region, within five PCR fragments, were selected and successfully used for mtDNA mixture quantification. For all SNPs quantified in this study, a linear relationship was observed between measured and expected mixture ratios. The average standard deviations of each of the seven SNPs fell within the expected 1-2% (for 10 replicate reactions). In conclusion, this mtDNA mixture quantification system is an alternative application of the pyrosequencing technology and is useful in forensic DNA analysis. Pyrosequencing has been shown to provide a very rapid, accurate and easy to use quantification system that can be used in forensic casework investigations to resolve and interpret major and minor mtDNA contribution from multiple individuals, determine heteroplasmy ratios and monitor contamination.marie.allen@genpat.uu.se

P-003
Reducing mtDNA sequencing efforts by half in forensic casework

Allen M,  Nilsson M, Calloway C, Divne A-M

Department of Genetics and Pathology, Rudbeck Laboratory, Uppsala University, Sweden

Mitochondrial DNA (mtDNA) sequencing can be time-consuming and laborious, limitations that can be minimized using a faster typing assay. The LINEAR ARRAY mtDNA HVI/HVII Region-Sequence Typing Kit (Roche Applied Science) uses sequence-specific probes immobilized in 31 lines. Linear array typing of mtDNA polymorphisms is a simple and fast pre-screening method with potential to substantially reduce sequencing efforts due to exclusion of samples. The analysis is performed in less than 3 hours without the need for expensive equipment.
Over a five-year period more than 300 forensic samples have been successfully typed for mtDNA polymorphisms using these linear arrays in our laboratory. A majority of the specimens that were analyzed using the combined HVI/HVII linear array were shed hairs. However, previous use of the HVII linear array has been successful on samples obtained from a variety of items, such as epithelial cells collected from areas in close contact with the skin. Furthermore, successful linear HVI/HVII array typing results have been obtained in a cold case investigation of 15-years old hair samples, one shed head hair (3 cm long) and two reference hairs.
A high sensitivity in the assay was shown by typing of TaqMan quantified DNA samples with limited amounts. Successful and reliable results were obtained from three centimetre pieces of distal shaft parts of shed and plucked hairs. Moreover, strong and easily interpretable array signals were obtained from control samples containing 100 -10 000 mtDNA copies, equivalent to 0.6 pg to 60 pg of genomic DNA (333 genome equivalents/ng DNA) indicating a highly sensitive typing system.
The exclusion capacity has been evaluated by a retrospective study of 90 previously HVI/HVII sequenced samples (57 evidence samples and 33 reference samples) from 16 forensic cases. Using the HVI/HVII mtDNA linear array, 56% of the samples were excluded and thus less than half of the samples require further sequencing due to a match or inconclusive results. Of all the samples that were excluded by sequence analysis, 79% could be excluded using the HVI/HVII linear array alone.
The use of the mtDNA linear arrays in our laboratory has served as a valuable pre-screening method and demonstrates the potential to reduce the required sequencing efforts by more than half. Thus, this rapid and user-friendly linear array typing system provides a convenient and efficient pre-screening method for selection of the samples of most interest for further investigation.

P-004
The Amelogenin locus displays a high frequency of X homologue failures in São Tomé island (West Africa)

Alves C1, Coelho M1, Rocha J1,2, Amorim A1,2

1 IPATIMUP, R. Dr. Roberto Frias, s/n, 4200-465 Porto, Portugal
2 Faculdade de Ciências da Universidade do Porto, Pr. Gomes Teixeira, 4009-002 Porto, Portugal

A multiplex STR study using the Powerplex 16 System (Promega) in 503 unrelated individuals from the island of São Tomé (Gulf of Guinea, West Africa) revealed 10 male individuals presenting only the Y homologue of the Amelogenin locus (~2%). These individuals were further typed with other commercial kits which also amplify the Amelogenin locus, namely the AmpFLSTR Identifler (Applied Biosystems) and Y-PlexTM12 (Reliagene) kits, and an X/Y genotype was only obtained with the primers used in Y-PlexTM12.
Although this X Amelogenin drop-out was only detected in males, this does not rule out the fact that females may also carry it. Since women have two X chromosomes, in some instances it could be suspected that an X failure was also present in females, by simple observation of differences in electrophoregram peak heights, in comparison with XY profiles. Although we cannot objectively consider these apparent nulls in females for frequency estimate purposes, there is no doubt of its magnitude in this population. With a 2% frequency in males, it is expected that the frequency of female carriers and homozygotes will be 3.92% and 0.04%, respectively. It is also noteworthy that the previously reported frequency for X Amelogenin null (which was estimated in Caucasians) was much lower (0.3%).
Failure to amplify alleles in the Amelogenin locus has been described before, mainly in cases where the Y homologue fails, which can have critical consequences in forensic casework. Cases where the X counterpart fails to amplify, as described here, are not of fundamental significance in forensic genetics, since there is no danger of a male individual being mistaken for a female one. However, this can have a different impact in other fields, such as in prenatal diagnosis of certain XY chromosome abnormalities, like XXY, using quantitative assays.
The high frequency of amplification failures already detected for either the X or Y chromosome Amelogenin locus, only draws our attention more to the need for caution when applying solely the amelogenin test for sex determination.
Sequencing of the X Amelogenin allele responsible for the amplification failure in the 10 male individuals is undergoing.


P-005
Making the most of Y-STR haplotypes. The HapYDive

Alves C1, Gusmão L1, Meirinhos J1, Amorim A1,2
1 IPATIMUP, R. Dr. Roberto Frias, s/n, 4200-465 Porto, Portugal; 2 Faculdade de Ciências da Universidade do Porto, Pr. Gomes Teixeira, 4009-002 Porto, Portugal

Since the informative power of a Y-STR marker can only be recognised in a haplotype context, a software was devised to evaluate the increase of haplotype diversity (HD) by the addition of any combination of markers to a fixed number of markers. The first version of the program was quite limited and not very user-friendly. The HapYDive is the latest version, created in Excel format (available at www.ipatimup.pt/app/). It´s not only a software for Y-STR HD calculation but, more importantly, it allows the determination of which combination of Y-STRs is the most informative in a certain population sample. With the HapYDive it is possible to analyse any set of Y markers up to a maximum of 20, with a minimum number of 4 markers fixed for calculations.
As an example, let’s consider the fixed set of Y-STRs currently used in the "YHRD - Y Chromosome Haplotype Reference Database" (http://www.yhrd.org), comprising the “minimal haplotype” markers (9 loci) plus DYS438 and DYS439. Depending on the population sample, these 11 loci together will have a certain HD value. Which set and what number of the other available Y-STRs will increase more rapidly the HD value?
Applying the HapYDive program to a population sample from Portugal (N=657) with haplotypes containing the 11 Y-STRs plus DYS437, DYS460, DYS461, DYS635, GATA A10 and GATA H4, the best order of markers is shown in Table 1. In this sample, all the other Y-STRs contribute to a certain degree to an increment of HD, but DYS460 contributes the most and DYS635 the least.
However, in other samples, particularly in those from different population groups, one or more Y-STRs may not contribute in any way, and the order in which they´ll contribute more may be quite different. For example, by applying the HapYDive to a population sample from Mozambique (N=112) using the same markers, the best order is shown in Table 2. In this case, the order is different and there is one marker, DYS437, that does not contribute in any way to a higher HD.
Apart from applying this program to different sample origins and to different sets of Y-STR markers (namely from the recent commercial kit Yfiler from Applied Biosystems), it is also worth studying the effect of sample size. This study is still undergoing and a discussion of the results will be shown. Contact: calves@ipatimup.pt
Table 1 (Portugal)


Table 2 (Mozambique)

Y-STR sets
HD

Y-STR sets
HD
11 Y-STRs
0.99771

11 Y-STRs
0.99212
11 Y-STRs + DYS460
0.99866

11 Y-STRs + GATA A10
0.99437
12 Y-STRs + GATA H4
0.99915

12 Y-STRs + DYS460
0.99582
13 Y-STRs + GATA A10
0.99936

13 Y-STRs + DYS635
0.99646
14 Y-STRs + DYS461
0.99950

14 Y-STRs + DYS461
0.99695
15 Y-STRs + DYS437
0.99960

15 Y-STRs + GATA H4
0.99727
16 Y-STRs + DYS635
0.99966

16 Y-STRs + DYS437
0.99727

P-006
Estimating the post-mortem interval (I)
The use of genetic markers to aid in identification of Dipteran species and subpopulations

Ames C, Turner B, Daniel B

Department of Forensic Science and Drug Monitoring, King’s College London, UK

Insect evidence can be utilised in a forensic investigation in a variety of ways. For instance, insects are most commonly used to help in the estimation of time since death of a discovered corpse. With a knowledge of recent environmental conditions of the scene of crime, an entomologist can predict how long it has taken for any insects present to have reached their particular developmental stage and hence the minimum time since death. The insect species present on a corpse will also indicate the time since death as insect species colonise a carcass in a distinct succession. Some insects have distinct geographical distributions, their presence outside of their normal habitat could indicate post mortem movement of a corpse or link a suspect to a scene of crime. Their lifecycles are seasonal and presence of insects can therefore indicate the time of year a crime occurred. The presence of drugs or poisons within feeding insects may give an indication of cause of death of a body.
All forensic entomology techniques depend upon accurate identification of insect species. At present this is mainly based upon morphological differences between species. This can be difficult as the early lifecycle stages of many forensically important Dipteran species are very hard to distinguish.
One aim of this work was to use DNA molecular markers to help in identification of forensically important fly species and ultimately populations within the UK.
Wild populations of Calliphora vicina and Calliphora vomitoria (Diptera: Calliphoridae) caught from various locations around the UK were raised and maintained in the laboratory. Both these species are early corpse invaders in the United Kingdom. To ensure the identity of both species before experimental work began, they were characterised morphologically using a key (Smith 1986). DNA was extracted from adults and larval forms. Regions of both the nuclear (xanthine dehydrogenase exon 2) and mitochondrial (cytochrome oxidase I and the control region) genomes were amplified using PCR and then sequenced or digested using restriction enzymes.
These molecular markers have been shown to contain both interspecific and intra specific variation and thus can be used to distinguish between the two species and also between English populations of both species.

Contact: carole.ames@kcl.ac.uk

P-007
Estimating the post-mortem interval (II) The use of differential temporal gene expression to determine the age of  blowfly pupae

Ames C, Turner B, Daniel B
Department of Forensic Science and Drug Monitoring, King’s College London, UK

Insect evidence can be utilised in a forensic investigation in a variety of ways. For instance, insects are most commonly used to help in the estimation of time since death of a discovered corpse. With a knowledge of recent environmental conditions of the scene of crime, an entomologist can predict how long it has taken for any insects present to have reached their particular developmental stage and hence the minimum time since death. The insect species present on a corpse will also indicate the time since death as insect species colonise a carcass in a distinct succession. Some insects have distinct geographical distributions, their presence outside of their normal habitat could indicate post mortem movement of a corpse or link a suspect to a scene of crime. Their lifecycles are seasonal and presence of insects can therefore indicate the time of year a crime occurred. The presence of drugs or poisons within feeding insects may give an indication of cause of death of a body.
To establish time since death, an entomologist requires accurate assessment of the age of insects discovered associated with a corpse. At present this is done using morphological features or biometric characteristics such as length or weight. The aim of this work was to use molecular techniques to determine the age of immature forms of forensically important fly species. Throughout the developmental lifecycle of insects different genes will be expressed at specific time points. Once identified these temporally expressed genes could provide markers as to the age of an insect.
Wild populations of Calliphora vicina (Diptera: Calliphoridae) were maintained in the laboratory. This species is an early corpse invader in the United Kingdom. Initially the pupal stage would be focussed upon. Adult females were encouraged to lay eggs and this was taken as ‘time zero’. Eggs were placed at a constant 20C until the pupal stage. At specific timepoints total RNA was extracted from pupal samples. The extracted mRNA was reverse transcribed to cDNA. Potential markers were located either from the use of differential display techniques (DD) or from the literature. DD is a method that detects changes in gene expression between samples by the random amplification of cDNA. Fragments are visualised on a gel and differences in banding pattern can be focussed upon.
Once potential markers were located their expression in differently aged pupal samples was quantified using Real-time PCR. The results indicated that this is a viable method for age determination of Dipteran immature stages.

P-008
Extended Northern Portuguese database on 21 autosomal STRs used in genetic identification

Amorim A1,2, Alves C1, Gusmão L1, Pereira L1
1IPATIMUP, R. Dr. Roberto Frias, s/n, 4200-465 Porto, Portugal;2Faculdade de Ciências da Universidade do Porto, Pr. Gomes Teixeira, 4009-002 Porto, Portugal

Routine casework in our genetic identification laboratory is carried out with two commercially available autosomal STR kits, namely Identifiler (Applied Biosystems) and Powerplex 16 (Promega), which together amplify a total of 17 STR loci. In some instances, namely in deficient paternity cases, we can also count on an in-house multiplex system which amplifies 4 more loci, totalling 21 STRs. Along the years, we have accumulated population frequency data in our database, namely from individuals residing in Northern Portugal, which we are now presenting extensively, together with parameters of forensic interest. This is also the first time we are presenting data on both D2S1338 and D19S433. The following table summarises our results:


CD4
(N=382)
CSF1PO
(N=1825)
D2S1338
(N=760)
D3S1358
(N=1816)
D5S818
(N=1816)
D7S820
(N=1809)
D8S1179
(N=1822)
Ho
0.696
0.731
0.833
0.784
0.702
0.794
0.808
He
0.705
0.724
0.877
0.787
0.702
0.810
0.811
PD
0.855
0.872
0.973
0.921
0.859
0.937
0.941
CE
0.422
0.452
0.741
0.556
0.436
0.601
0.616
P
0.929
0.496
0.798
0.754
0.597
0.112
0.034


D13S317
(N=1818)
D16S539
(N=1283)
D18S51
(N=1810)
D19S433
(N=761)
D21S11
(N=1817)
F13A01
(N=484)
FES
(N=487)
Ho
0.773
0.760
0.891
0.806
0.843
0.711
0.700
He
0.782
0.776
0.876
0.794
0.843
0.754
0.700
PD
0.922
0.915
0.972
0.930
0.957
0.899
0.852
CE
0.566
0.546
0.733
0.587
0.673
0.509
0.417
P
0.495
0.760
0.919
0.820
0.552
0.098
0.818


FGA
(N=1833)
MBPB
(N=371)
Penta D
(N=1280)
Penta E
(N=1281)
TH01
(N=2403)
TPO
(N=2402)
VWA
(N=2303)
Ho
0.857
0.741
0.837
0.899
0.783
0.639
0.804
He
0.866
0.728
0.839
0.885
0.796
0.648
0.810
PD
0.967
0.879
0.953
0.976
0.927
0.823
0.937
CE
0.712
0.469
0.657
0.755
0.570
0.386
0.602
P
0.316
0.360
0.015
0.786
0.658
0.691
0.915
N: nº individuals; Ho: observed heterozygosity; He: expected heterozygosity according to Nei; PD: power of discrimination; CE: a priori chance of exclusion; P: Hardy-Weinberg equilibrium, exact test based on more than 2000 shufflings, for standard error <0.01.

Deviations from Hardy-Weinberg equilibrium were detected in D8S1179 and Penta D loci, but applying the Bonferroni correction for the number of loci analysed, the departure in both loci was not significant (0.05/21=0.0024).
Both commercial STR kits share 13 loci but use different primer pairs, and so genotype inconsistencies may occur. For individuals genotyped as homozygotes with one kit and as heterozygotes with the other, the latter genotype was the one considered.
The overall matching probability for the 21 STRs in our population sample is of 1 in 1.56 x 1024 individuals, and combined power of exclusion of 0.9999999914.

P-009
Evaluation of the 11 Y-STR loci in the PowerPlex® Y-system;
Experience from analyses of single male samples and simple male: male mixtures.

Andreassen R, Heitman IK

Institute of Forensic Medicine, University of Oslo, Norway

Interpretation of sample mixtures requires knowledge about the efficiency of the system. In this study we have measured the amount of stutter and pull-up in 100 male samples analysed at 11 Y-STR loci (DYS 391, DYS389I/II, DYS 439, DYS 393, DYS 390, DYS 385, DYS 438, DYS 437, DYS 19, DYS 392) using the PowerPlex® Y-system as described by the manufacturer. The proportion of stutter differed among the loci in the multiplex-kit and was associated with allele length (number of repeats) and repeat size (3-5 basepairs). The best performing locus was DYS 438 while largest proportion of stutter was observed in locus DYS 389II. Area of stutter was less than 0.2 for all loci tested. Both stutter in position N-2 and N+1 was observed at certain loci. No pull up larger than 0.1 was observed in the loci analysed. Locus DYS 393 was amplified less efficient than other loci in the multiplex mix giving alleles with low peak heights compared to the others. Efficiency for each Y-STR locus will be presented in detail. Fourteen samples from males with known Y-haplotypes were used to compose male:male mixtures. Mixture ratios varied within the interval 1:3 to 1:1. A total of sixty-five samples were analysed. In each sample the peak areas of alleles were used to type a “minor” and a “major” Y-haplotype consisting of all minor alleles or major alleles, respectively, at loci with two alleles. The results from this exercise were compared with the two known Y-haplotypes in each sample. Disregarding locus DYS 393 and DYS 385 a/b, the two Y-haplotypes in a sample was correctly typed in all samples with a relative peak area difference (average of peak areas of minor alleles / peak area of major alleles) less than 0.6. The results from this simple test indicate that peak area of alleles in PowerPlex® Y-system provides quantitative information that might be used to interpret the most likely Y-haplotypes in a simple male:male mixture.

E-mail:                                r.j.andreassen@medisin.uio.no



P-010
Icelandic population data for the 10 autosomal STR loci in the AMPFlSTR®SGM Plus™ system and the 11 Y-STR loci in the PowerPlex® Y-system

Andreassen R, Heitman IK, Hansen L, Mevaag B

Institute of Forensic Medicine, University of Oslo, Norway

Autosomal STR polymorphisms at 10 loci (D3S1358, vWA, D16S539, D21S1338, D8S1179, D21S11, D18S51, D19S433, TH01 and FGA) and Y-STR polymorphisms at 11 loci (DYS 391, DYS389I/II, DYS 439, DYS 393, DYS 390, DYS 385, DYS 438, DYS 437, DYS 19, DYS 392) are presented. Samples from a population material of unrelated individuals from Iceland were analysed using the AMPFlSTR®SGM Plus™ system (n=110) and the PowerPlex® Y-system (n=76) as described by the manufacturer. For the autosomal polymorphisms the observed heterozygosities ranged from 0,764 (vWA) to 0,891 (FGA). No significant deviation from Hardy-Weinberg equilibrium was observed. For the Y-chromosome polymorphisms 62 different haplotypes were observed in the 76 male samples analysed. No haplotype was observed more than three times in the population sample.
Locus diversity, allele distributions and other relevant forensic genetic parameters will be presented in detail.



E-mail:                                r.j.andreassen@medisin.uio.no

P-011
Low Copy Number: interpretation of evidence results

Anjos MJ1, Andrade L1, Carvalho M1, Lopes V1, Serra A1, Oliveira C1, Balsa F1, Brito P1, Corte-Real F2, Vide MC1

1 Forensic Genetic Service. National Institute of Legal Medicine. Largo da Sé Nova, 300 Coimbra. Portugal
2 National Institute of Legal Medicine. Largo da Sé Nova, 300 Coimbra. Portugal
geneforense@dcinml.mj.pt


Evidence of crime scene and samples from decomposed or skeletal remains have in many cases, low amounts or degraded DNA.
The choice of extraction protocols as well as sensitive and robust STR’s is crucial to obtain good results but in many situations is not enough; it is necessary to make protocol adaptations of amplification instructions even when are used commercial kits.
One of the most common modifications is changing the number of cycles in the amplification protocol, with an increment of 4, 6 or more cycles. However in some cases there are difficulties in interpreting results because extra peaks appear or an imbalance between them seems to have no sense.
In this work we show some cases where changes of technical approaches produced better results and others where we had problems in interpreting evidence results.


P-012

Amelogenin as a Target for Real Time PCR Quantitation of Forensic Templates


Anwar N, Goodman M, Hulme P, Elsmore P, Greenhalgh M and McKeown B

Orchid BioSciences (Europe) Ltd, Abingdon, UK

PCR is the ubiquitous method of forensic DNA analysis, but prior to amplification, two other processes are crucial to obtaining a satisfactory result: template DNA extraction and template quantitation.  Here we will presume the extraction process has been performed, and concentrate on the quantitation step: a focus of recent advances.  Real time quantitative PCR (RT-QPCR) is an advantageous alternative to probe hybridisation or fluorescent dye association, which are (respectively) laborious and less accurate procedures.  We reviewed the available commercial methods of RT-QPCR and concluded that for our requirements, a more attractive solution was the in-house development and validation of an ultra-rapid, small batch size solution.  Our solution is  real time detection using the Roche LightCycler 2.0 and the amplification of a 106/112bp amelogenin amplicon.  Melt-curve analysis and back extrapolation to the starting template-dependant crossing point generates results from 32 samples in ~30 minutes (post PCR assembly) and this approach has advantages in that a positive quantitation result implies that in the SGM Plusä amplification that follows, at the very least, an amelogenin product should be generated.  The use of the amelogenin target also provides an indication of the possibility of PCR product travelling from the separate PCR product room backwards into the clean PCR set-up environment, something that the use of telomerase or  b-globin amplicons cannot provide.  We have validated the use of our LightCycler-amelogenin based quantitation system and have seen significant improvements in the reliability of quantitation measurements in our forensic laboratories.
email: nanwar@orchid.co.uk , bmckeown@orchid.co.uk

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